GB425728A - Improvements in a method of preserving glycol ethers - Google Patents

Improvements in a method of preserving glycol ethers

Info

Publication number
GB425728A
GB425728A GB1393334A GB1393334A GB425728A GB 425728 A GB425728 A GB 425728A GB 1393334 A GB1393334 A GB 1393334A GB 1393334 A GB1393334 A GB 1393334A GB 425728 A GB425728 A GB 425728A
Authority
GB
United Kingdom
Prior art keywords
ether
glycol ethers
preserving
triethanolamine
alkali
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB1393334A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HENRY LEON COX
Carbide and Carbon Chemicals Corp
Original Assignee
HENRY LEON COX
Carbide and Carbon Chemicals Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HENRY LEON COX, Carbide and Carbon Chemicals Corp filed Critical HENRY LEON COX
Priority to GB1393334A priority Critical patent/GB425728A/en
Publication of GB425728A publication Critical patent/GB425728A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/46—Use of additives, e.g. for stabilisation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Glycol ethers, especially the mono and dialkyl ethers of alkylene and polyalkylene 1,2 glycols, are stabilized by adding a small quantity of a hydroxyalkylamine such as triethanolamine. If aldehydes are present, the ether is preferably first treated by refluxing with acid, neutralizing with alkali, and distilling under reduced pressure. In an example, the monoethyl ether of ethylene glycol is refluxed for 5 hours with a small quantity of sulphuric acid, then a slight excess of alkali is added, and the mixture is fractionated, after which 0,1 per cent of triethanolamine is added to the purified ether.
GB1393334A 1934-05-08 1934-05-08 Improvements in a method of preserving glycol ethers Expired GB425728A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB1393334A GB425728A (en) 1934-05-08 1934-05-08 Improvements in a method of preserving glycol ethers

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB1393334A GB425728A (en) 1934-05-08 1934-05-08 Improvements in a method of preserving glycol ethers

Publications (1)

Publication Number Publication Date
GB425728A true GB425728A (en) 1935-03-20

Family

ID=10032008

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1393334A Expired GB425728A (en) 1934-05-08 1934-05-08 Improvements in a method of preserving glycol ethers

Country Status (1)

Country Link
GB (1) GB425728A (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2481278A (en) * 1946-08-31 1949-09-06 Shell Dev Polyoxyalkylene compounds
US2492955A (en) * 1946-08-31 1950-01-03 Shell Dev Polyoxyalkylene compounds
US2514982A (en) * 1946-10-18 1950-07-11 Shell Dev Stabilized lubricant
US2624708A (en) * 1950-06-23 1953-01-06 Union Carbide & Carbon Corp Inhibited polyoxyalkylene glycol fluids
US2665312A (en) * 1951-08-03 1954-01-05 Dow Chemical Co Stabilized polyglycol compositions
US2687378A (en) * 1951-12-11 1954-08-24 California Research Corp Lubricating oil composition
US2687377A (en) * 1951-12-11 1954-08-24 California Research Corp Lubricant
US3294734A (en) * 1961-04-13 1966-12-27 Hoechst Ag Amine stabilized trioxane copolymers

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2481278A (en) * 1946-08-31 1949-09-06 Shell Dev Polyoxyalkylene compounds
US2492955A (en) * 1946-08-31 1950-01-03 Shell Dev Polyoxyalkylene compounds
US2514982A (en) * 1946-10-18 1950-07-11 Shell Dev Stabilized lubricant
US2624708A (en) * 1950-06-23 1953-01-06 Union Carbide & Carbon Corp Inhibited polyoxyalkylene glycol fluids
US2665312A (en) * 1951-08-03 1954-01-05 Dow Chemical Co Stabilized polyglycol compositions
US2687378A (en) * 1951-12-11 1954-08-24 California Research Corp Lubricating oil composition
US2687377A (en) * 1951-12-11 1954-08-24 California Research Corp Lubricant
US3294734A (en) * 1961-04-13 1966-12-27 Hoechst Ag Amine stabilized trioxane copolymers

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