US934833A - Separating apparatus. - Google Patents

Description

'H. G. PARKER. SEPARATING APPARATUS.

APPLICATION FILED JAN,9,1908.

Patented Sept. 21, 1909.

l jmWegaW/Ka HARRY G. mimmo or LIBERY; Mismo-Rr Srirfiimriim Arriiiii'ris.

(fifty-in the County of Slay and SCatefo Mis; of the stziml yoke mii zi' portion of lche Myinvenio relfat'e's to" a separatfixigappshaft' a'ii'dddmpt ci for revolution ratus, and more particularly to an apparatus 0 eri' Spfice ii ei l'he yoke ai' ii' i o'c' that cla-Ss forA use iii chemical analysis W 'el.' glouifni'ed'm a box Soli base i 15 wherein the' Sepfr'ation' of a preoipitize is ltezii'lly projeofiug shiff "I, ligiving e, ,gear

i311v the separation of :i precipitate iii quarl- #he gari-oiisliufi and' n crank 9 oo iis oni ria'tive chemical analysis it has Ordinarily enel Wiiereby the parte are' operated. L been the custom to pass the liquid containing' topz oi1v shaft 3 iw idly mouned i fue i 1M the precipitate through a filer of paper, asfroirz opposite' de 'of Whi'oli are 'eil bestos, orother like material, which filter is the' n'rihs' 1.1.7 ne ng'iili'y Secured to the, o'ui'er afterward' either ireighed with the precipieii'rls o f sh'id arrhsii're the Semicii'jeuizrr oraciotate, :mdsllowance made therefora or the lei's'a'l2; tl'ieiio miki' paris chrieceffi thorefilter is borne@ before the We'iglfiais taken'. ,iitlibeing (iupiica'es of en ii other; for In either oase the precipicfre must' be in mwhich reason but on# will hereafter be redied before ille Wei ht is taken,v Which to? ieii to the iorlf; with the, under- `@ether with the inoicV ent exposure lio the air, Staiifl'iiig ihaft Siiiidesoripiion refers equily presents an opportunity 'for ioss in trims? 'to both, Projeeying ihwarniiy from @he eh'fi fi ieri-ing, and oxidation, or from other ea'uses. of the brieliec i2 re he yi' "i'`5.,1i} oii" which l-t is ille object of' my' invention to prois irminioneii ir rin'g und projecting; vi'f'l'e alu zipparm'us wherein' the solili'on may tlu'ogii sairl, rimjiss'zi ji L51 having a Geiler be heated :md precipitation ziceoiiiplished 1G adapted fo seni :if iet ami support the ilhouf removal from theoriginal container, jl 'fl'm lig i4: l .fomhly fiiog Wihiri iromwvhioh the liquid'nmy lie reiiio'vei'if'er jfr l5' is' a chlziiner i?, preferabiy of he preeipiiaio, :md inv which the precipiace less'eiier oon'ierfer shape, Whioh preerl 1i1z1"y be weighed before' being lfiariiieiE and :ibly slip-ported" on' :ui informed iii ge ifi,

40 Withoutoxposiire to the air," zuidI Without p'reiferbiy formeii iniegrzii yriiir L corr the use of the usual filter. lIi aloeompiish ziiiii: The oontiihr 7 iSpi'oiiide'ilwi/i'h fi 25.5 irre?y this; ooieet I limite u'se of aii'or'diiiry IllllV which is nlliipted io fit Siiugly Wiiir ceutriugi'.maehinefsueh asis u'seinrlialrin or close to the n iouth .of a receptcie `Q0 ing butter falo' determinatios and a" spe'oiziii Wlieir the loiterifests iieotly pri ih e hoioixji claims, reference being had to tlie" ztoco'iii d' fi. rilbhrf like sleeel for #he por pzi'nyi'u'g drawings, iii which like' reference pSe i4 piiiieniin'g lakig'e through the umerl's refer to like parts throughot` the joint.V 5@ several-views, and in Whioll: operation) the liquid coiigaip'iig the . y ceases guided by the sloping sides of the container into a receptaclel `Where it is highly cornpressed by the force. After all the precipitate has been thrown down', the liquor may be removed by decanting,'siphon1ng, or pour' ing as desired. Should any. particles of the precipitate adhere to the sides of the con-v tainer they may be loosened by a swabber inI troduced through the mouth of the container.'

If it should be desired to wash the precipi tate in soine gas, or in a solution of some gas, the gas or solution may be introduced into the .container and corked in. Then When whirled the precipitate or other compound in the container passes through the solut-ion of the gas and is Washed by it.

In case it should be desired to heat, cook, or boil some precipitate yor compound the Whole jar and container could be placed over the burner and the Water introduced between the jar and coiitainei-woiild act like the Water cushion in the ordinary Water bath, and the precipitate could be heated, ete., Without being removed :from the original receptacle, `and the container in no more danger of f breaking than fiasks, etc.,- in the ordinary i baths. The Water cushion serves to equalize the pressure inside the container and recep-A tacle, to prevent leakage and to 'render possible the use or" a comparatively fragile material for container and receptacle. The level i of the Water cushion may be slightly higher than thelevel of the liquid in the container', so that the liow will be slightly inward thus Washing the joint between the c ontainer and the receptacle from any portion of the precipitating liquid.

Having thus described my invention, What I claim as new ,therein and desire to secure by Letters Patent is l. In a separating apparatus, a container having a necl, and a detachable precipitate receptacle adapted to lit over said neck, for the purpose set forth.

9.. ln a separating apparatus, a solution container having a neck at one end, a detachable precipitate receptacle adapted for adjustment on said neck, means for holding said receptacle to said neck, and means for revolving said container and receptacle l around a common center, for the purpose set forth.

3. In a separating apparatus, a solution container having a neck, a detachable pre'- cipitate receptacle adaptedto iitv over said neclr, a collar adapted` to engage a portion o'f said container and said receptacle, and

means for revolving said parts, for the purpose set forth.

4. ln a separating apparatus, a solution v container having a neck, a detachable precipitate .receptacle adapted to fit over said neck, and an elastic collar adapted to encentrifugal machine. The precipitate bein g gage a portion of said container and a pot*- lorced outward by the centrifugal force 1s tion of said receptacle, for the-n purpose set' forth. l l

5. In a separating'apparatus, a suitable jar, a solution container adapted to fit Within said jar and having a detachable precipitate exit port,and a precipitate receptacle adapti ed to seat Within saidjar and cover the exit port in said container, substantially as setl vforth.

6. ln a' separating apparatus, a suitable -jar, asolution container adapted to lit Within Asaid jar and having a detachable precipitate exit port, .a precipitate receptacle adapted to seat on the bottom of said jar and having a mouth adapted to cover said exit port, substantially as and for the purpose set forth.

7. In a separating apparatus, a. suitable jar, a solution container adapted to lit within receptacle, substantially as and for the pury pose set forth.

8. `In a separating apparatus, a jar having an -internal flange, a solution container located Within said jar and seated against said iiange, a precipitate. receptacle seated on the bottom of said jar, and a neck on said container projecting into said receptacle, substantially as and for the purpose set forth. I

9. Ina separating apparatus, a jar having an internal flange, a solution receptacle located Within said jarand seated against said iiange, a detachable precipitate receptacle seated on the bottom of said jar, a neck on said container projecting into said receptacle, and means for actuating said jar, for the purpose set forth.

10. A separating apparatus comprising a centrifugal mechanism, a suitable jar carcentrifugal mechanism,- a precipitate recep tacle, and a solution receptacle having converging sides terminating iii said precipitate receptacle, said receptacle being adapted for attachment to and detachment :troni saidv container'. i

i2. A separating apparatus comprising-a 'centrifugal mechanism, a lWater tight device adapted vt'or carrying ay solution container and a precipitate receptacle, a receptacle carricd thereby, and a container carried by said device and provided' with converging sides terminating insaid, receptacle, said recepdetachment from si'd container, -S'ubStansaid jar,4 and a precptterreceptabcle heatedn saidjar and connecfg with "Sad sjoution 'containerg'both the' QQ faze being surroulndejby @Momma 1p said jar, said receptaclebeng adapt-d for f attachment to and detachment from sawhimper, Substantially as set forth.

, In 'tefstimony whereof I afHX my .signfatureY

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